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Comparative Study of Microwave Assisted and Conventional Synthesis of Tp*-Complexes

Received: 20 January 2018     Accepted: 8 February 2018     Published: 28 February 2018
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Abstract

Cobalt, copper and nickel complexes with tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate (Tp*) were synthesized by the reaction of potassium tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate (KTp*) with the corresponding metal(II) chloride by using conventional reflux methods and microwave methods. The two methods were compared and the microwave method was found to be less time consuming and gave higher yields.

Published in Journal of Photonic Materials and Technology (Volume 4, Issue 1)
DOI 10.11648/j.jmpt.20180401.14
Page(s) 19-25
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2018. Published by Science Publishing Group

Keywords

Pz* [3,5-dimethyl-1H-pyrazol-1-yl], KTp* [potassium tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate], Tp*-complexes, [tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate complexes]

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  • APA Style

    Hamed Aboajila Alqamoudy, Hussain Ibrahim Alarabi. (2018). Comparative Study of Microwave Assisted and Conventional Synthesis of Tp*-Complexes. Journal of Photonic Materials and Technology, 4(1), 19-25. https://doi.org/10.11648/j.jmpt.20180401.14

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    ACS Style

    Hamed Aboajila Alqamoudy; Hussain Ibrahim Alarabi. Comparative Study of Microwave Assisted and Conventional Synthesis of Tp*-Complexes. J. Photonic Mater. Technol. 2018, 4(1), 19-25. doi: 10.11648/j.jmpt.20180401.14

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    AMA Style

    Hamed Aboajila Alqamoudy, Hussain Ibrahim Alarabi. Comparative Study of Microwave Assisted and Conventional Synthesis of Tp*-Complexes. J Photonic Mater Technol. 2018;4(1):19-25. doi: 10.11648/j.jmpt.20180401.14

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  • @article{10.11648/j.jmpt.20180401.14,
      author = {Hamed Aboajila Alqamoudy and Hussain Ibrahim Alarabi},
      title = {Comparative Study of Microwave Assisted and Conventional Synthesis of Tp*-Complexes},
      journal = {Journal of Photonic Materials and Technology},
      volume = {4},
      number = {1},
      pages = {19-25},
      doi = {10.11648/j.jmpt.20180401.14},
      url = {https://doi.org/10.11648/j.jmpt.20180401.14},
      eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.jmpt.20180401.14},
      abstract = {Cobalt, copper and nickel complexes with tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate (Tp*) were synthesized by the reaction of potassium tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate (KTp*) with the corresponding metal(II) chloride by using conventional reflux methods and microwave methods. The two methods were compared and the microwave method was found to be less time consuming and gave higher yields.},
     year = {2018}
    }
    

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    AU  - Hamed Aboajila Alqamoudy
    AU  - Hussain Ibrahim Alarabi
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    T2  - Journal of Photonic Materials and Technology
    JF  - Journal of Photonic Materials and Technology
    JO  - Journal of Photonic Materials and Technology
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    UR  - https://doi.org/10.11648/j.jmpt.20180401.14
    AB  - Cobalt, copper and nickel complexes with tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate (Tp*) were synthesized by the reaction of potassium tris(3,5-dimethyl-1H-pyrazol-1-yl)hydroborate (KTp*) with the corresponding metal(II) chloride by using conventional reflux methods and microwave methods. The two methods were compared and the microwave method was found to be less time consuming and gave higher yields.
    VL  - 4
    IS  - 1
    ER  - 

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Author Information
  • Chemistry Department, Faculty of Science, Zawia University, Az Zawiyah, Libya

  • Chemistry Department, Faculty of Science, Zawia University, Az Zawiyah, Libya

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